4-氯-4'-羟基二苯甲酮合成路线 (共 30 条)
参考文献
Gharda Chemicals Limited
Patent: EP1903024 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
in dimethyl sulfoxide
参考文献
Orchimed S.A.
Patent: US4072705 A1, 1978 ;
反应条件
potassium hydroxide in water; dimethyl sulfoxide T=60°C; 18 h;
参考文献
Ridd, John H.; Yousaf, Taher I.; Rose, John B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
反应条件
1: AlCl3 / nitrobenzene 2: aq. HBr; AcOH View Scheme
参考文献
Malik; Saharia
Journal of Scientific and Industrial Research, 1956 , vol. 15 B, p. 633
反应条件
1: AlCl3 / nitrobenzene 2: aq. HBr; AcOH View Scheme
参考文献
Kurosu, Michio; Narayanasamy, Prabagaran; Biswas, Kallolmay; Dhiman, Rakesh; Crick, Dean C.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 17 p. 3973 - 3975
反应条件
aluminium trichloride 0.0833333 h;
参考文献
Nunes, R.C.; Diaz-Calleja, R.; Pinto, M.; Saiz, E.; Riande, E.
Journal of Physical Chemistry, 1995 , vol. 99, # 34 p. 12962 - 12970
反应条件
hydrogen bromide; acetic acid
参考文献
Kurosu, Michio; Narayanasamy, Prabagaran; Biswas, Kallolmay; Dhiman, Rakesh; Crick, Dean C.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 17 p. 3973 - 3975
反应条件
1: 45 percent / trifluoromethylsulphonic acid / 144 h 2: KOH / H2O; dimethylsulfoxide / 18 h / 60 °C View Scheme
参考文献
Ridd, John H.; Yousaf, Taher I.; Rose, John B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
反应条件
ethanol; sulfuric acid; sodium nitrite
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1920 , vol. 39, p. 345
Recueil des Travaux Chimiques des Pays-Bas, 1922 , vol. 41, p. 717
反应条件
aluminium trichloride
参考文献
Massolini; Carmellino; Baruffini
Farmaco, Edizione Scientifica, 1986 , vol. 41, # 5 p. 381 - 387