5-氯-1,10-菲咯啉合成路线 （共 11 条）
反应条件
diarsenic pentoxide; sulfuric acid
参考文献
Bock, H.; Haenel, P.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 2 p. 288 - 300
反应条件
1: 70 percent / hypochlorous acid, NaOAc, NaCl, 40percent Bu4NOH, pH = 6.5 / H2O; CHCl3 / 0.25 h / 0 °C 2: 97.5 percent / sodium metal / propan-2-ol / 0 deg C - RT, 1 h View Scheme
参考文献
Antkowiak, Roza; Antkowiak, Wieslaw Z.
Tetrahedron Letters, 1997 , vol. 38, # 10 p. 1857 - 1858
反应条件
hydrogenchloride T=165°C;
参考文献
Kuczynski; Sucharda
Roczniki Chemii, 1936 , vol. 16, p. 513,515
Chem. Zentralbl., 1937 , vol. 108, # I p. 3141
反应条件
1: 30 g / As2O5*5H2O, H2SO4 / 6 h / 130 °C 2: SnCl2*2H2O, 38percent HCl 3: 3 g / As2O5*5H2O, H2SO4 / 6 h / 130 °C View Scheme
参考文献
Bock, H.; Haenel, P.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 2 p. 288 - 300
反应条件
1: SnCl2*2H2O, 38percent HCl 2: 3 g / As2O5*5H2O, H2SO4 / 6 h / 130 °C View Scheme
参考文献
Bock, H.; Haenel, P.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 2 p. 288 - 300
参考文献
Kuczynski; Sucharda
Roczniki Chemii, 1936 , vol. 16, p. 513,515
Chem. Zentralbl., 1937 , vol. 108, # I p. 3141
反应条件
T=21.85°C; Equilibrium constant;
参考文献
Nabavizadeh, S. Masoud
Dalton Transactions, 2005 , # 9 p. 1644 - 1648
反应条件
T=21.85°C; Equilibrium constant;
参考文献
Nabavizadeh, S. Masoud
Dalton Transactions, 2005 , # 9 p. 1644 - 1648
反应条件
1: KOH, Cu / 8 h / 160 °C / 18387.7 Torr 2: 1 g / H2SO4, HNO3 / 2 h View Scheme
参考文献
Druey; Schmidt
Helvetica Chimica Acta, 1950 , vol. 33, p. 1080,1085
反应条件
1: HMPA / 2.5 h / 120 °C
2: aq. HCl
View Scheme
参考文献
Pozzo, Jean-Luc; Samat, Andre; Guglielmetti, Robert; Keukeleire, Denis De
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 7 p. 1327 - 1332
