1H-吡咯-3,4-二甲酰氯合成路线 （共 3 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in toluene
T=85°C; 0.833333 h;
参考文献
Kaesler, Ralph W.; LeGoff, Eugene
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4399 - 4402
反应条件
1: 95 percent / NaOH / ethanol; H2O / 2 h / Heating
2: oxalyl chloride, DMF / toluene / 0.83 h / 85 °C
View Scheme
参考文献
Kaesler, Ralph W.; LeGoff, Eugene
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4399 - 4402
反应条件
1: 97 percent / ammonium acetate / aq. ethanol / 24 h / Heating
2: 95 percent / NaOH / ethanol; H2O / 2 h / Heating
3: oxalyl chloride, DMF / toluene / 0.83 h / 85 °C
View Scheme
参考文献
Kaesler, Ralph W.; LeGoff, Eugene
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4399 - 4402
