2-乙酰基-4’-氯二苯硫醚合成路线 （共 5 条）
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide) T=50°C; 16 h;
参考文献
Anderson, Steven N.; Bhatia, Pramila A.; Kolasa, Teodozyj; Nakane, Masaki; Patel, Meena V.; Rohde, Jeffrey J.; Zhiren, Xia; Zhang, Henry Qing-Wei
Patent: US2004/192680 A1, 2004 ;
Location in patent: Page 14; 15 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Anderson, Steven N.; Bhatia, Pramila; Kolasa, Teodozyj; Nakane, Masaki; Patel, Meena V.; Rohde, Jeffrey J.; Xia, Zhiren; Zhang, Henry Q.
Patent: US2004/121994 A1, 2004 ;
反应条件
(i) Mg, EtOH, CCl4, Et2O, (ii) /BRN= 2696447/, (iii) aq. H2SO4, AcOH; Multistep reaction;
参考文献
Jilek,J.O. et al.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 115 - 131
反应条件
1: sulfur / 150 - 160 °C 2: KOH / ethanol 3: Na<AlH2(OCH2CH2OMe)2> / benzene View Scheme
参考文献
Jilek,J.O. et al.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 115 - 131
反应条件
1: sulfur / 150 - 160 °C
2: KOH / ethanol
View Scheme
参考文献
Jilek,J.O. et al.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 115 - 131
