1-甲基-2-(4-甲基苯基)磺酰基-苯合成路线 （共 20 条）
反应条件
1,10-phenanthroline; 4 A molecular sieve; oxygen; copper diacetate in dichloromethane; dimethyl sulfoxide
T=40°C; 72 h; atmospheric pressure;
参考文献
Huang, Fang; Batey, Robert A.
Tetrahedron, 2007 , vol. 63, # 32 p. 7667 - 7672
反应条件
potassium carbonate; palladium dichloride in acetone
T=25°C; Suzuki-Miyaura reaction; 1 h;
参考文献
Bandgar; Bettigeri, Sampada V.; Phopase, Jaywant
Organic Letters, 2004 , vol. 6, # 13 p. 2105 - 2108
反应条件
potassium acetate in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Shen, Chao; Xu, Jun; Yu, Wenbo; Zhang, Pengfei
Green Chemistry, 2014 , vol. 16, # 6 p. 3007 - 3012
反应条件
aluminium trichloride in dichloromethane
T=25°C; Rate constantProduct distribution;
参考文献
DeHaan, Franklin P.; Ahn, Paul Y.; Kemnitz, Carl R.; Ma, Steven K.; Na, Jim; Patel, Bimal R.; Ruiz, Richard M.; Villahermosa, Randy M.
International Journal of Chemical Kinetics, 1998 , vol. 30, # 5 p. 367 - 372
反应条件
aluminium trichloride
T=25°C; Acylation; 0.75 h;
参考文献
Ghiaci; Asghari
Synthetic Communications, 1998 , vol. 28, # 12 p. 2213 - 2220
反应条件
iron(III) chloride
T=110°C; 0.166667 h; microwave irradiation; Title compound not separated from byproducts.;
参考文献
Marquie; Laporterie; Dubac; Roques; Desmurs
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 421 - 425
反应条件
trifluoromethylsulfonic anhydride in tetrachloroethane, 1,1,2,2-
T=120°C; 12 h; Title compound not separated from byproducts.;
参考文献
Yao, Bangben; Zhang, Yuhong
Tetrahedron Letters, 2008 , vol. 49, # 37 p. 5385 - 5388
反应条件
1: NMPTsO With TPPD in dichloromethane
0.5 h;
2: toluene in dichloromethane
T=0 - 20°C; 2 h; Overall yield = 80 percent; chemoselective reaction;
参考文献
Khodaei; Nazari
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 4 p. 507 - 512
反应条件
Benzoesaeure-fluorsulfonsaeureanhydrid in dichloromethane
T=0°C; 14 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Huthmacher, Klaus; Keil, Michael
Chemische Berichte, 1981 , vol. 114, # 5 p. 1967 - 1971
反应条件
SbF5; epoxysulfonyl fluoride
T=0°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Tanaka, Mutsuo; Souma, Yoshie
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3738 - 3740
