三甲基(对甲苯乙炔)硅烷合成路线 (共 36 条)
参考文献
Journal of Organometallic Chemistry, , vol. 395, # 2 p. 227 - 229
反应条件
copper(l) iodide; palladium; triphenylphosphine; aluminum oxide; potassium fluoride Sonogashira coupling reaction; 0.0416667 h; microwave irradiation;
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
反应条件
N-iodo-succinimide; silver nitrate in N,N-dimethyl-formamide 24 h; Darkness;
参考文献
Shi, Yu; Li, Xiaoyu; Liu, Jianhui; Jiang, Wenfeng; Sun, Licheng
Tetrahedron Letters, 2010 , vol. 51, # 28 p. 3626 - 3628
反应条件
water; triethylamine; triphenylphosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=160°C; P=51485.6 Torr; 4 h;
参考文献
Takeuchi, Ryo; Yasue, Hiroyuki
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5386 - 5392
反应条件
piperidine; bis-triphenylphosphine-palladium(II) chloride
T=70°C; 0.166667 h;
参考文献
Leadbeater, Nicholas E.; Tominack, Bonnie J.
Tetrahedron Letters, 2003 , vol. 44, # 48 p. 8653 - 8656
反应条件
diisopropylammonium bromide; [(t-Bu)3PH]BF4; copper(l) iodide; Na2[PdCl4] in various solvent(s)
T=80°C; Sonogashira coupling; 20 h;
参考文献
Koellhofer, Axel; Plenio, Herbert
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 9 p. 1295 - 1300
反应条件
proton-exchanged montmorillonite in 1,4-dioxane
T=100°C; 5 h; Inert atmosphere;
参考文献
Motokura, Ken; Matsunaga, Shigekazu; Miyaji, Akimitsu; Yashima, Tatsuaki; Baba, Toshihide
Tetrahedron Letters, 2011 , vol. 52, # 50 p. 6687 - 6692
反应条件
zinc(II) chloride in 1,4-dioxane
T=100°C; 1.5 h;
参考文献
Andreev, Aleksey A.; Konshin, Valeri V.; Komarov, Nikolai V.; Rubin, Michael; Brouwer, Chad; Gevorgyan, Vladimir
Organic Letters, 2004 , vol. 6, # 3 p. 421 - 424
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
1 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
zinc trifluoromethanesulfonate; triethylamine in dichloromethane
T=23°C; 12 h;
参考文献
Rahaim Jr., Ronald J.; Shaw, Jared T.
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2912 - 2915