lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether Cooling with iceRefluxInert atmosphere;
参考文献
SANOFI-AVENTIS; PALUMED S.A.; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S.)
Patent: US2012/122923 A1, 2012 ;
Location in patent: Page/Page column 17 ;