4'-乙酰苯并-15-冠-5-醚合成路线 （共 13 条）
反应条件
methanesulfonic acid; phosphorous pentoxide T=20°C; 6 h;
参考文献
Paramonov, Sergey V.; Lokshin, Vladimir; Smolentsev, Artem B.; Glebov, Evgeni M.; Korolev, Valeri V.; Basok, Stepan S.; Lysenko, Konstantin A.; Delbaere, Stephanie; Fedorova, Olga A.
Tetrahedron, 2012 , vol. 68, # 38 p. 7873 - 7883
反应条件
PPA in acetic acid T=60°C;
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
sodium hydroxide in butan-1-ol
参考文献
Sakata, Kazunori; Shimoda, Manabu; Hashimoto, Mamoru
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1593 - 1598
反应条件
1: 60 percent 2: 70 percent / 1.) P2O5, MeSO3H; 2.) polyphosphoric acid / acetic acid View Scheme
参考文献
Zhao, Liyan; Xia, Wujiong; Gou, Baoquan; Lu, Yu; Yang, Chao; Li, Dazhi
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 95, p. 199 - 203
反应条件
K10 clay; copper dichloride 1.) 200 deg C; 2.) 52 deg C, 3 h;
参考文献
Cseri, Tivadar; Bekassy, Sandor; Bodas, Zoltan; Agai, Bela; Figueras, Francois
Tetrahedron Letters, 1996 , vol. 37, # 9 p. 1473 - 1476
反应条件
1: 60 percent 2: 70 percent / 1.) P2O5, MeSO3H; 2.) polyphosphoric acid / acetic acid View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
2: 80 percent / polyphosphoric acid / acetic acid / 60 °C View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
1: pyridine; thionyl chloride / benzene 2: water; sodium hydroxide / butan-1-ol / Inert atmosphere 3: Eaton’s reagent View Scheme
参考文献
Zhao, Liyan; Xia, Wujiong; Gou, Baoquan; Lu, Yu; Yang, Chao; Li, Dazhi
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 95, p. 199 - 203
反应条件
sodium acetate in acetic acid Irradiation;
参考文献
Tada, Masaru; Hirano, Hideki; Suzuki, Atsushi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 8 p. 2304 - 2308
反应条件
aluminium trichloride Yield given. Multistep reaction;
参考文献
Cseri, Tivadar; Bekassy, Sandor; Bodas, Zoltan; Agai, Bela; Figueras, Francois
Tetrahedron Letters, 1996 , vol. 37, # 9 p. 1473 - 1476
