[(1-甲基乙基)亚磺酰]-苯合成路线 (共 14 条)
反应条件
ethylmagnesium bromide; diisopropylamine 1.) Et2O, 0 deg C, 20 min, 2.) Et2O, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 9 p. 2645 - 2647
反应条件
water; Nitrous oxide Ambient temperatureIrradiationpH:2;
参考文献
Veltwisch, Dieter; Janata, Eberhard; Asmus, Klaus-Dieter
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 146 - 153
反应条件
N-chloro-succinimide; silica gel 20 h; Ambient temperature;
参考文献
Drabowicz, Jozef
Synthesis, 1986 , # 10 p. 831 - 833
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=0 - 20°C; 1 h;
参考文献
Tetrahedron, , vol. 51, # 9 p. 2699 - 2708
反应条件
ziconium(IV) oxychloride octahydrate; sodium iodide in water T=90°C; 2.3 h; chemoselective reaction;
参考文献
Jafarpour, Maasoumeh; Rezaeifard, Abdolreza; Heidari, Mahdieh
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 7 p. 1470 - 1482
反应条件
ethylmagnesium bromide; diisopropylamine in diethyl ether
3 h; Ambient temperature;
参考文献
Kobayashi, Kazuhiro; Kawakita, Masataka; Yokota, Kouichi; Mannami, Tohru; Yamamoto, Koji; et al.
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 5 p. 1401 - 1408
反应条件
ethylmagnesium bromide; diisopropylamine; p-chlorobenzenethiol in diethyl ether
Ambient temperature;
参考文献
Kobayashi, Kazuhiro; Kawakita, Masataka; Akamatsu, Hideki; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 9 p. 2645 - 2647
反应条件
diisopropylamine
1.) Et2O, 0 deg C, 1 h, 2.) Et2O, RT, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kobayashi, Kazuhiro; Yokota, Kouichi; Akamatsu, Hideki; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 2 p. 441 - 443
反应条件
ethylmagnesium bromide; diisopropylamine
1.) Et2O, 0 deg C, 20 min, 2.) Et2O, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kobayashi, Kazuhiro; Kawakita, Masataka; Akamatsu, Hideki; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 9 p. 2645 - 2647
反应条件
ethylmagnesium bromide; diisopropylamine
1.) Et2O, 0 deg C, 20 min, 2.) Et2O, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kobayashi, Kazuhiro; Kawakita, Masataka; Akamatsu, Hideki; Morikawa, Osamu; Konishi, Hisatoshi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 9 p. 2645 - 2647