N-水杨酰-N'-苯甲酰肼合成路线 （共 9 条）
反应条件
thionyl chloride T=78°C; 6 h;
参考文献
Tandon; Doval; Shanker; Sinha
Pharmazie, 1982 , vol. 37, # 5 p. 388 - 389
反应条件
1: anhydrous sodium benzoate; benzoyl chloride in chloroform
T=5 - 22°C;
2: salicyloylhydrazine in chloroform
参考文献
Liu, Shi-Xiong; Lin, Shen; Lin, Bi-Zhou; Lin, Chi-Chang; Huang, Jian-Quan
Angewandte Chemie - International Edition, 2001 , vol. 40, # 6 p. 1084 - 1087
反应条件
methanesulfonic acid in acetonitrile
Heating;
参考文献
Lee; Kim; Cho
Synthesis, 1992 , # 10 p. 929 - 930
反应条件
in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Zhao, He; Burke Jr., Terrence R.
Tetrahedron, 1997 , vol. 53, # 12 p. 4219 - 4230
反应条件
methanesulfonic acid in toluene
4 h; Heating;
参考文献
Lee; Kim; Cho
Synthesis, 1992 , # 10 p. 929 - 930
反应条件
1: 50 percent / DCC / dioxane / Ambient temperature
2: 75 percent / dimethylformamide / Ambient temperature
View Scheme
参考文献
Zhao, He; Burke Jr., Terrence R.
Tetrahedron, 1997 , vol. 53, # 12 p. 4219 - 4230
参考文献
Koz'minykh; Goncharov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 6 p. 864 - 867
参考文献
Koz'minykh; Goncharov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 6 p. 864 - 867
反应条件
1: 98percent hydrazine hydrate / methanol / 10 h / Heating
2: 76 percent / 8 h / 145 - 150 °C
View Scheme
参考文献
Tandon; Doval; Shanker; Sinha
Pharmazie, 1982 , vol. 37, # 5 p. 388 - 389
