反应条件
1: 93 percent / aq. H2SO4 / 12 h / 140 °C
2: 1.) POCl3 / 1.) 0 deg C, 15 min, 2.) 60 deg C, 10 h
3: 78.6 percent / NaBH4 / propan-2-ol
4: 25 g / HBr(g) / benzene; petroleum ether / -15 °C
5: NaI / acetone / 72 h / Ambient temperature
View Scheme
参考文献
Fatope; Abraham
Journal of Medicinal Chemistry, 1987 , vol. 30, # 11 p. 1973 - 1977
