N-甲基-4-硝基邻苯二甲酰亚胺合成路线 (共 18 条)
反应条件
N,N-dimethyl-formamide T=125 - 130°C;
参考文献
Billman; Cash
Proceedings of the Indiana Academy of Science, 1953 , vol. 63, p. 108
反应条件
sodium chloride; HEG-Cl in toluene T=120°C; Inert atmosphereReflux; Product distribution / selectivity;
参考文献
SABIC Innovative Plastics IP B.V.
Patent: US2009/292128 A1, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogenchloride; water; tin(ll) chloride T=20°C;
参考文献
Duan, Xin-Hong; Qiao, Jin-Ping; Yang, Yang; Cui, Meng-Chao; Zhou, Jiang-Ning; Liu, Bo-Li
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 3 p. 1337 - 1343
参考文献
University of Kentucky Research Foundation
Patent: US7759468 B1, 2010 ;
反应条件
1.1: toluene; dimethyl sulfoxide / 140 - 160 °C
1.2: 6 h / 120 °C
2.1: water; sodium hydroxide / 24 h / |Reflux
View Scheme
参考文献
Rajasekar; Venkatesan
Polymer (United Kingdom), 2013 , vol. 54, # 21 p. 5626 - 5633
反应条件
biphenyl; triethylamine in isobutyramide
参考文献
General Electric Company
Patent: US4625037 A1, 1986 ;
反应条件
biphenyl; triethylamine in toluene
参考文献
GENERAL ELECTRIC COMPANY
Patent: EP172298 B1, 1991 ;
反应条件
N-neopentyl chloride of 4-dibutylaminopyridine in toluene
T=110°C; 1 h;
参考文献
Brunelle, D. J.; Singleton, Daniel A.
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3383 - 3386