苯胺-2,3,4,5,6-d5合成路线 （共 28 条）
反应条件
palladium 10 on activated carbon; ammonium formate in methanol 0.333333 h; Inert atmosphereReflux;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 53, # 3 p. 148 - 152
反应条件
copper(I) oxide; ammonium hydroxide in 1-methyl-pyrrolidin-2-one T=80°C; 15 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 22 p. 9098 - 9101
反应条件
1: With platinum on carbon; hydrogen; water-d2 T=80°C; 24 h; 2: With water in diethyl ether
参考文献
Bulletin of the Chemical Society of Japan, , vol. 81, # 2 p. 278 - 286
反应条件
1: 87 percent / HNO3; H2SO4 / 0.75 h / 60 °C 2: 73 percent / Sn; conc. HCl / 1 h / Heating View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 41, # 12 p. 1103 - 1126
参考文献
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, , vol. 38, # 8 p. 903 - 912
反应条件
hydrogenchloride; zinc
参考文献
Chemische Berichte, , vol. 118, # 5 p. 1782 - 1797
反应条件
1: 85 percent / 0.5 h / Heating 2: 70 percent / SOCl2; AlCl3 / CS2 / 6 h / Heating 3: 70 percent / 30 percent H2O2 / acetic acid / Heating View Scheme
参考文献
Gannett, Peter M.; Johnson II, Edward M.; Grimes, Michael A.; Myers, Alan L.; Deavers III, Robert E.; Tracy, Timothy S.
Journal of Labelled Compounds and Radiopharmaceuticals, 2003 , vol. 46, # 2 p. 107 - 114
反应条件
1: 85 percent / 0.5 h / Heating 2: 70 percent / SOCl2; AlCl3 / CS2 / 6 h / Heating 3: 70 percent / 30 percent H2O2 / acetic acid / Heating 4: 80 percent / 10 percent DCl / 2.5 h / Heating View Scheme
参考文献
Gannett, Peter M.; Johnson II, Edward M.; Grimes, Michael A.; Myers, Alan L.; Deavers III, Robert E.; Tracy, Timothy S.
Journal of Labelled Compounds and Radiopharmaceuticals, 2003 , vol. 46, # 2 p. 107 - 114
反应条件
tri-tert-butyl phosphine; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) in toluene 3 h; Heating / reflux;
参考文献
LG CHEM, LTD.
Patent: WO2007/108666 A1, 2007 ;
Location in patent: Page/Page column 38 ;
反应条件
1: in diethyl ether 1 h; 2: With sodium acetate; acetic anhydride T=90°C; 2 h;
参考文献
HOPITAL SAINTE-JUSTINE
Patent: WO2005/12247 A1, 2005 ;
Location in patent: Page/Page column 27-28 ;
