1-(1-甲基乙基)-2-苯基-氮丙啶合成路线 （共 8 条）
参考文献
Capriati, Vito; Florio, Saverio; Luisi, Renzo; Musio, Biagia
Organic Letters, 2005 , vol. 7, # 17 p. 3749 - 3752
反应条件
zinc(II) chloride in 1,2-dichloro-ethane
T=80°C; 1 h;
参考文献
Kuehnau, Dorte; Thomsen, Ib; Jorgensen, Karl Anker
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 11 p. 1167 - 1170
反应条件
PPh3.Br2; triethylamine in acetonitrile
参考文献
Piotti, Marcelo E.; Alper, Howard
Journal of the American Chemical Society, 1996 , vol. 118, # 1 p. 111 - 116
反应条件
toluene-4-sulfonic acid in toluene
84 h; Heating;
参考文献
Tsuchiya, Yukiko; Kumamoto, Takuya; Ishikawa, Tsutomu
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8504 - 8505
反应条件
1: styrene With bromo-dimethylsulfonium bromide in acetonitrile
0.166667 h; Cooling with ice;
2: isopropylamine in water
T=20°C;
参考文献
Yang, Zhen-Zhen; Li, Yu-Nong; Wei, Yang-Yang; He, Liang-Nian
Green Chemistry, 2011 , vol. 13, # 9 p. 2351 - 2353
反应条件
Bu2SnClH-HMPA
1.) THF, r.t., 3 h, 2.) 40 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kawakami, Takayo; Sugimoto, Takayuki; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo; Sonoda, Noboru
Journal of Organic Chemistry, 1995 , vol. 60, # 9 p. 2677 - 2682
反应条件
1: acetonitrile / 0.17 h / Cooling with ice
2: water / 20 °C
View Scheme
参考文献
Dou, Xiao-Yong; He, Liang-Nian; Yang, Zhen-Zhen
Synthetic Communications, 2012 , vol. 42, # 1 p. 62 - 74
反应条件
lithium aluminium tetrahydride in diethyl ether
7 h; Heatingvarious molar ratios, solvents, time. Other N-alkyl- and N-aryltrichloroacetophenone imines; Product distribution;
参考文献
Kimpe, Norbert De; Verhe, Roland; Buyck, Laurent De; Schamp, Niceas
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2079 - 2081
