1,2,3,4,6-O-五乙酰基-Alpha-甘露糖合成路线 （共 76 条）
反应条件
hydrogenchloride; acetyl chloride T=-70°C;
参考文献
Korytnyk; Mills
Journal of the Chemical Society, 1959 , p. 636,644
反应条件
1: With trimethylsilyl iodide in dichloromethane
0.5 h; Heating;
2: With tetra-N-butylammonium azide in dichloromethane
0.166667 h;
参考文献
Ying, Laiqiang; Gervay-Hague, Jacquelyn
Carbohydrate Research, 2003 , vol. 338, # 9 p. 835 - 841
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=20°C; 24 h;
参考文献
Wu, Shanshan; Huang, Xuan; Du, Xuezhong
Angewandte Chemie - International Edition, 2013 , vol. 52, # 21 p. 5580 - 5584
Angew. Chem., 2013 , vol. 125, # 21 p. 5690 - 5694,5
反应条件
1: 77 percent / BF3*OEt2 / CH2Cl2 / 16 h / Heating
2: MeONa / methanol / 1 h / 20 °C / pH 7
View Scheme
参考文献
Daly, Robin; Vaz, Gisela; Davies, Anthony M.; Senge, Mathias O.; Scanlan, Eoin M.
Chemistry - A European Journal, 2012 , vol. 18, # 46 p. 14671 - 14679
反应条件
trimethylsilylazide; silver perchlorate; tin(IV) chloride in dichloromethane; toluene
5 h;
参考文献
Matsubara, Koki; Mukaiyama, Teruaki
Chemistry Letters, 1994 , # 2 p. 247 - 250
反应条件
1: I2; triethylsilane / CH2Cl2 / Heating
2: sodium borohydride / acetonitrile / 20 °C
View Scheme
参考文献
Adinolfi, Matteo; Iadonisi, Alfonso; Ravida, Alessandra; Schiattarella, Marialuisa
Tetrahedron Letters, 2003 , vol. 44, # 43 p. 7863 - 7866
