6,7-二氢-5H-环戊并[b]吡啶-7-醇合成路线 （共 5 条）
反应条件
potassium hydroxide in ethanol T=20°C; 1 h;
参考文献
Pereira, Cidaliasilva; Salgado, Sofia; Rizzo-Aguiar, Fabio; Garcia-Mera, Xerardo; Rodriguez-Borges, Josee.
Synlett, 2013 , vol. 24, # 7 art. no. ST-2012-D1091-L, p. 837 - 838
反应条件
1: With trifluoroacetic anhydride in dichloromethane T=0 - 20°C; 16 h; 2: With lithium hydroxide in dichloromethane; water T=20°C; 16 h;
参考文献
Pereira, Cidaliasilva; Salgado, Sofia; Rizzo-Aguiar, Fabio; Garcia-Mera, Xerardo; Rodriguez-Borges, Josee.
Synlett, 2013 , vol. 24, # 7 art. no. ST-2012-D1091-L, p. 837 - 838
反应条件
1.1: mCPBA / CH2Cl2 / 16 h / 20 °C 2.1: trifluoroacetic anhydride / CH2Cl2 / 16 h / 0 - 20 °C 2.2: lithium hydroxide / CH2Cl2; H2O / 16 h / 20 °C View Scheme
参考文献
Pereira, Cidaliasilva; Salgado, Sofia; Rizzo-Aguiar, Fabio; Garcia-Mera, Xerardo; Rodriguez-Borges, Josee.
Synlett, 2013 , vol. 24, # 7 art. no. ST-2012-D1091-L, p. 837 - 838
反应条件
sulfuric acid T=130°C;
参考文献
Robison
Journal of the American Chemical Society, 1958 , vol. 80, p. 6254,6255
反应条件
Dess-Martin periodane in dichloromethane
参考文献
Andreotti, Daniele; Miserazzi, Emanuele; Nalin, Arnaldo; Pozzan, Alfonso; Profeta, Roberto; Spada, Simone
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6526 - 6530
