water; chlorine 1.) DMFA, from 60 to 70 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Avdeenko, A. P.; Velichko, N. V.; Tolmachev, A. A.; Pirozhenko, V. V.; Romanenko, E. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 1 p. 146 - 154
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 1 p. 136 - 143
1: 1.) gaseous chlorine, 2.) H2O / 1.) DMFA, from 60 to 70 deg C 2: 87 percent / hydrochloric acid, gaseous chlorine / dimethylformamide View Scheme
参考文献
Avdeenko, A. P.; Velichko, N. V.; Tolmachev, A. A.; Pirozhenko, V. V.; Romanenko, E. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 1 p. 146 - 154
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 1 p. 136 - 143
water; chlorine 1.) DMFA, from 60 to 70 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Avdeenko, A. P.; Velichko, N. V.; Tolmachev, A. A.; Pirozhenko, V. V.; Romanenko, E. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 1 p. 146 - 154
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 1 p. 136 - 143
bromine in N,N-dimethyl-formamide
T=30°C; other N,N'-bis(arylsulfonyl)-1,4-benzoquinonediimines, other solvents: CCl4, CHCl3, acetic acid presence, other reaction temperatures; MechanismProduct distribution;
参考文献
Avdeenko, A. P.; Velichko, N. V.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 2 p. 221 - 225
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 2 p. 249 - 254