2,2-二甲基-1,3-二氧戊环-4-酮合成路线 （共 14 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 0.5 h;
2: With water; sodium sulfate in tetrahydrofuran
T=0 - 20°C; 2 h;
参考文献
Hashimoto, Masaya; Iwasawa, Yoshikazu; Kawamoto, Hiroshi; Ohta, Hisashi; Ozaki, Satoshi; Sagara, Takeshi; Sakoh, Hiroki; Satoh, Atsushi
Patent: US2007/15792 A1, 2007 ;
Location in patent: Page/Page column 11 ;
反应条件
in toluene
18 h; Heating;
参考文献
Khalaj, A.; Nahid, E.
Synthesis, 1985 , # 12 p. 1153 - 1155
反应条件
in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Daryaee, Fereidoon; Kobarfard, Farzad; Khalaj, Ali; Farnia, Parisa
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 1 p. 289 - 295
反应条件
in toluene
14 h; Heating;
参考文献
Boyko, Vyacheslav I.; Rodik, Roman V.; Severenchuk, Inna N.; Voitenko, Zoya V.; Kalchenko, Vitaly I.
Synthesis, 2007 , # 14 p. 2095 - 2096
