反应条件
chloro-trimethyl-silane; Ti(iso-propylate)[(tris(2-hydroxy-3,5-dimethylbenzyl)amine)(-3H)]; cyclohexa-1,4-diene; magnesium in tetrahydrofuran
T=40 - 50°C; 24 h; Inert atmosphere; Reagent/catalyst; Overall yield = 99 percent; regioselective reaction;
参考文献
Takekoshi, Naoto; Miyashita, Kenji; Shoji, Noriaki; Okamoto, Sentaro
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2151 - 2157