反应条件
in dichloromethane under N2, PhBBr2 in CH2Cl2 droped to a soln. of Sn-compound at -78°C under stirring, warmed to room temp.; volatiles removed at room temp. and 1E-2 Torr, Et2SnBr2 sublimed at 25°C and 5E-6 Torr, residue recrystd. (CH2Cl2); elem. anal.;
参考文献
Franz, Thomas; Hanecker, Elisabeth; Noeth, Heinrich; Stoecker, Walter; Storch, Wolfgang; Winter, Gerhard
Chemische Berichte, 1986 , vol. 119, # 3 p. 900 - 916
