2-甲基-3-(吡咯烷-1-基)丙酸甲酯合成路线 (共 6 条)
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Moffett
Journal of Organic Chemistry, 1949 , vol. 14, p. 862,866
Org. Synth. Coll., 1963 , vol. Vol. IV, p. 834
反应条件
hydrogen fluoride T=7 - 8°C; 8.08333 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.5 V - 6.7 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
反应条件
hydrogen fluoride T=7 - 8°C; 8.08333 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.5 V - 6.7 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202
反应条件
iodine in dichloromethane
T=20°C; Aza-Michael addition; 0.416667 h;
参考文献
Borah, Kalyan Jyoti; Phukan, Mridula; Borah, Ruli
Synthetic Communications, 2010 , vol. 40, # 19 p. 2830 - 2836
反应条件
in tetrahydrofuran; methanol
Heating;
参考文献
Anjaiah, Siddam; Chandrasekhar, Srivari; Gree, Rene
Tetrahedron Letters, 2004 , vol. 45, # 3 p. 569 - 571
反应条件
hydrogen fluoride
T=7 - 8°C; 8.08333 h; electrochemical reaction; anodic current density of 3.5 A dm-2, a cell voltage of 6.5 V - 6.7 V; Further byproducts given;
参考文献
Abe, Takashi; Fukaya, Haruhiko; Hayashi, Eiji; Hayakawa, Yoshio; Nishida, Masakazu; Baba, Hajime
Journal of Fluorine Chemistry, 1994 , vol. 66, # 2 p. 193 - 202