6-氯-2-甲基苯并噻唑合成路线 （共 20 条）
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one; toluene T=20°C; 17 h; Inert atmosphere; chemoselective reaction;
参考文献
Malhotra, Sushant; Seng, Pamela S.; Koenig, Stefan G.; Deese, Alan J.; Ford, Kevin A.
Organic Letters, 2013 , vol. 15, # 14 p. 3698 - 3701
反应条件
hydrogenchloride in ethylene glycol 7 h; Heating;
参考文献
Nivalkar, Kishor R.; Mashraqui, Sabir H.
Synthetic Communications, 1996 , vol. 26, # 19 p. 3535 - 3542
反应条件
sodium hydroxide; potassium hexacyanoferrate(III)
参考文献
Tabakovic,I. et al.
Synthesis, 1979 , p. 590 - 592
反应条件
1: pyridine / 2 h / 120 °C 2: phosphorus pentasulfide / benzene / 3 h / Heating 3: NaH / toluene / 0.5 h / Heating View Scheme
参考文献
Van Zandt, Michael C.; Jones, Michael L.; Gunn, David E.; Geraci, Leo S.; Jones, J. Howard; Sawicki, Diane R.; Sredy, Janet; Jacot, Jorge L.; DiCioccio, A. Thomas; Petrova, Tatiana; Mitschler, Andre; Podjarny, Alberto D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 9 p. 3141 - 3152
反应条件
1: phosphorus pentasulfide / benzene / 3 h / Heating 2: NaH / toluene / 0.5 h / Heating View Scheme
参考文献
Van Zandt, Michael C.; Jones, Michael L.; Gunn, David E.; Geraci, Leo S.; Jones, J. Howard; Sawicki, Diane R.; Sredy, Janet; Jacot, Jorge L.; DiCioccio, A. Thomas; Petrova, Tatiana; Mitschler, Andre; Podjarny, Alberto D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 9 p. 3141 - 3152
反应条件
in methanol 20 h; Irradiation;
参考文献
Paramasivam, R.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 930 - 934
反应条件
in methanol 24 h; Irradiation;
参考文献
Paramasivam, R.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 930 - 934
参考文献
Clarke,K. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 356 - 359
反应条件
1: 73 percent / P2S5 / benzene / Heating 2: 69 percent / methanol / 24 h / Irradiation View Scheme
参考文献
Paramasivam, R.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 930 - 934
反应条件
1: 75 percent / P2S5 / benzene / Heating 2: 84 percent / methanol / 20 h / Irradiation View Scheme
参考文献
Paramasivam, R.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 930 - 934
