1-(1-羟基苯基)-3-(4-甲氧基苯基)丙烷-1,3-二酮合成路线 (共 12 条)
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 5.5 h; Further byproducts given;
参考文献
Nishinaga, Akira; Maruyama, Kazushige; Ando, Hiroyuki; Sato, Ryoji; Mashino, Takahiro; Inada, Akira; Nakanishi, Tsutomu
Tetrahedron Letters, 1990 , vol. 31, # 22 p. 3171 - 3174
反应条件
triethylamine in ethanol Ambient temperature; Mechanism;
参考文献
Joglekar, S. J.; Samant, S. D.
Tetrahedron Letters, 1988 , vol. 29, # 2 p. 241 - 244
反应条件
gallium trifluoromethanesulfonate in nitromethane T=80°C; 2 h;
参考文献
Su; Zhu; Li
Organic Preparations and Procedures International, 2009 , vol. 41, # 1 p. 69 - 75
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 5.5 h; Further byproducts given;
参考文献
Nishinaga, Akira; Maruyama, Kazushige; Ando, Hiroyuki; Sato, Ryoji; Mashino, Takahiro; Inada, Akira; Nakanishi, Tsutomu
Tetrahedron Letters, 1990 , vol. 31, # 22 p. 3171 - 3174
反应条件
thiophosphoryl trichloride; water; triethylamine T=30 - 80°C; 0.333333 h;
参考文献
Vimal, Manorama; Pathak, Uma; Pandey, Lokesh Kumar; Suryanarayana, Malladi V. S.
Synthesis, 2011 , # 1 p. 30 - 32
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 5.5 h; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 31, # 22 p. 3171 - 3174
参考文献
Fletcher et al.
Tetrahedron Letters, 1959 , # 6 p. 9
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 5.5 h; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 31, # 22 p. 3171 - 3174
反应条件
1: With sulfuric acid; ammonium chloride; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water
3 h;
2: With toluene-4-sulfonic acid in dimethyl sulfoxide
T=50 - 60°C; 1 h;
参考文献
Makrandi; Shashi; Kumar, Surender
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 895 - 896
反应条件
sulfuric acid; ammonium chloride; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water
3 h;
参考文献
Makrandi; Shashi; Kumar, Surender
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 895 - 896