3’,4’-二甲氧基黄酮合成路线 （共 40 条）
反应条件
iodine in dimethyl sulfoxide 0.0333333 h; Microwave irradiation;
参考文献
Mcnczcs; Manjrckar; Pai; Patrc; Tilvc
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 9 p. 1311 - 1314
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane T=0 - 40°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Yoshida, Masahito; Fujino, Yuta; Doi, Takayuki
Organic Letters, 2011 , vol. 13, # 17 p. 4526 - 4529
反应条件
iodine T=100 - 110°C; 1.4 h; Neat (no solvent);
参考文献
Sashidhara, Koneni V.; Kumar, Manoj; Kumar, Abdhesh
Tetrahedron Letters, 2012 , vol. 53, # 18 p. 2355 - 2359
反应条件
iron(III) chloride in dichloromethane T=20°C; 1 h;
参考文献
Kucukislamoglu, Mustafa; Nebioglu, Mehmet; Zengin, Mustafa; Arslan, Mustafa; Yayli, Nurettin
Journal of Chemical Research, 2005 , # 9 p. 556 - 557
反应条件
selenium(IV) oxide in 3-methyl-1-butanol T=140 - 150°C; 14 h;
参考文献
Ahmed; Khan; Alam
Pharmazie, 2003 , vol. 58, # 3 p. 173 - 176
反应条件
potassium carbonate in N,N-dimethyl-formamide T=125°C; 24 h; Inert atmospheresealed tube;
参考文献
Zhao, Jie; Zhao, Yufen; Fu, Hua
Organic Letters, 2012 , vol. 14, # 11 p. 2710 - 2713
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Ullmann type reaction; 1 h; under air;
参考文献
Zhao, Jie; Zhao, Yufen; Fu, Hua
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3769 - 3773
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Ullmann type reaction; 1.5 h; under air;
参考文献
Zhao, Jie; Zhao, Yufen; Fu, Hua
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3769 - 3773
反应条件
1: pyridine 2: KOH / Heating 3: glacial acetic acid; H2SO4 / 100 °C View Scheme
参考文献
Maki, Yoshifumi; Shimada, Kaoru; Sako, Magoichi; Hirota, Kosaku
Tetrahedron, 1988 , vol. 44, # 11 p. 3187 - 3194
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=0 - 67°C; 2: With sulfuric acid in acetic acid 2.5 h; Heating; Further stages.;
参考文献
McKendall, Michael; Smith, Tasha; Anh, Kien; Ellis, Jamie; McGee, Terri; Foroozesh, Maryam; Zhu, Naijue; Stevens, Cheryl L. Klein
Journal of Chemical Crystallography, 2008 , vol. 38, # 4 p. 231 - 237
