2-氨基-N-甲基苯甲酰胺合成路线 （共 35 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; Inert atmosphereReflux;
2: With sodium hydroxide in tetrahydrofuran; water
1 h; Inert atmosphere;
参考文献
Paleta, Oldrich; Dolensky, Bohumil; Palecek, Jiri; Kvicala, Jaroslav
European Journal of Organic Chemistry, 2013 , # 7 p. 1262 - 1270
反应条件
di-tert-butyl peroxide; toluene-4-sulfonic acid
T=110°C; 20 h; Schlenk technique;
参考文献
Zhao, Dan; Wang, Teng; Li, Jian-Xin
Chemical Communications, 2014 , vol. 50, # 49 p. 6471 - 6474
反应条件
1: 96 percent / ethanol / 0 °C
2: conc. hydrochloric acid / ethanol / 3 h / Heating
View Scheme
参考文献
Knape
Journal fuer Praktische Chemie (Leipzig), 1891 , vol. <2> 43, p. 213,217
反应条件
C{N(2,6-iPr2C6H3)CH}2
T=70°C; 24 h;
参考文献
Jacquet, Olivier; DasNevesGomes, Christophe; Ephritikhine, Michel; Cantat, Thibault
ChemCatChem, 2013 , vol. 5, # 1 p. 117 - 120
反应条件
2 h; Heating; Yield given;
参考文献
Gravier; Dupin; Casadebaig; Hou; Boisseau; Bernard
European Journal of Medicinal Chemistry, 1989 , vol. 24, # 5 p. 531 - 535
参考文献
Schoepf; Oechler
Justus Liebigs Annalen der Chemie, 1936 , vol. 523, p. 1,26
反应条件
palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt in water
T=120°C; 16 h; sealed tube;
参考文献
Hikawa, Hidemasa; Ino, Yukari; Suzuki, Hideharu; Yokoyama, Yuusaku
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7046 - 7051
反应条件
aluminum oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone
Condensation; oxidation; 0.15 h; microwave irradiation;
参考文献
Santa Deepthi; Sahadeva Reddy; Reddy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 3 p. 220 - 222
反应条件
oxygen in dimethyl sulfoxide
T=120°C; 48 h;
参考文献
Kim, Na Yeun; Cheon, Cheol-Hong
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2340 - 2344
反应条件
diphenyl-phosphinic acid; oxygen in 1,4-dioxane
T=130°C; P=760.051 Torr; 18 h; Schlenk technique;
参考文献
Chen, Xiuling; Chen, Tieqiao; Zhou, Yongbo; Han, Daoqing; Han, Li-Biao; Yin, Shuang-Feng
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 23 p. 3802 - 3807
