2-羟基-1-(4-甲氧基苯基)-1-乙酮合成路线 （共 46 条）
反应条件
sodium ethanolate in ethanol
参考文献
Kaspersen, Svein Jacob; Hoff, Bard Helge; Sundby, Eirik; Charnock, Colin
Bioorganic Chemistry, 2012 , vol. 44, p. 35 - 41,7
反应条件
1: in aq. buffer Sonication; 2: in aq. buffer 1.5 h; IrradiationInert atmosphere;
参考文献
Jayaraj, Nithyanandhan; Jagadesan, Pradeepkumar; Samanta, Shampa R.; Da Silva, Jose P.; Ramamurthy
Organic Letters, 2013 , vol. 15, # 17 p. 4374 - 4377
反应条件
1: in aq. buffer Sonication; 2: in aq. buffer 1.5 h; IrradiationInert atmosphere;
参考文献
Jayaraj, Nithyanandhan; Jagadesan, Pradeepkumar; Samanta, Shampa R.; Da Silva, Jose P.; Ramamurthy
Organic Letters, 2013 , vol. 15, # 17 p. 4374 - 4377
反应条件
1: 2-hydroxy-1-(4-methoxy-phenyl)-ethanone With triethylamine in dichloromethane 24 h; Heating; 2: ethanethioamide With potassium carbonate in acetonitrile 10 h; Heating; Further stages.;
参考文献
Liu, Xiao-Ling; Wang, Qiu-Ying; Sheng, Shou-Ri; Xu, Chen; Cai, Ming-Zhong
Synthetic Communications, 2008 , vol. 38, # 19 p. 3338 - 3345
反应条件
sodium hydroxide in methanol; water T=20 - 30°C; var. solv.: DMF, DMSO and water; Mechanism;
参考文献
Morozov, A. A.
Russian Journal of Physical Chemistry, 1984 , vol. 58, # 12 p. 1823 - 1826
Zhurnal Fizicheskoi Khimii, 1984 , vol. 58, p. 3006 - 3009
反应条件
lithium hydroxide Multistep reaction;
参考文献
Morozov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 1.2 p. 215 - 222,186 - 192
反应条件
pyridine Yield given;
参考文献
Kovach, Ildiko M.; Zhao, Qinjian; Keane, Matthew; Reyes, Rachel
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10471 - 10476
反应条件
in methanol T=20 - 30°C; Mechanism;
参考文献
Morozov, A. A.
Russian Journal of Physical Chemistry, 1984 , vol. 58, # 12 p. 1823 - 1826
Zhurnal Fizicheskoi Khimii, 1984 , vol. 58, p. 3006 - 3009
反应条件
1: triethylamine / dichloromethane / 20 °C / Inert atmosphere 2: Ni(PCy3)2Cl2; sodium t-butanolate / N,N-dimethyl-formamide; toluene / 0.67 h / 100 °C / Inert atmosphere View Scheme
参考文献
Huang, Kun; Li, Gang; Huang, Wei-Ping; Yu, Da-Gang; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 25 p. 7224 - 7226
反应条件
manganese(IV) oxide in dichloromethane oxidation-Wittig reaction; 1 h; Heating;
参考文献
Runcie, Karen A.; Taylor, Richard J. K.
Chemical Communications, 2002 , # 9 p. 974 - 975
