2-烯丙基-1,2-苯并异噻唑-3(2H)-酮 1,1-二氧化物合成路线 (共 7 条)
反应条件
sodium hydroxide in N,N-dimethyl-formamide
0.5 h; Heating;
参考文献
Mabrour, Mahmoud; Bougrin, Khalid; Benhida, Rachid; Loupy, Andre; Soufiaoui, Mohamed
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 443 - 447
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; Mitsunobu Displacement; regioselective reaction;
参考文献
Wang, Xiaolong; Ma, Yanying; Ju, Tingting
Journal of Chemical Research, 2013 , vol. 37, # 7 p. 417 - 419
反应条件
[(PPh3)3Pd] in N,N-dimethyl-formamide
T=100°C; 5 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Toyofuku, Masanori; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3021 - 3022
参考文献
Abe
Yakugaku Zasshi, 1955 , vol. 75, p. 159,162
Chem.Abstr., 1956 , p. 1779
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Rice; Pettit
Journal of the American Chemical Society, 1943 , vol. 76, p. 302
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Hamor; Soine
Journal of the American Pharmaceutical Association (1912-1977), 1954 , vol. 43, p. 120,122
Full Text Show Details
Merritt; Levey; Cutter
Journal of the American Chemical Society, 1939 , vol. 61, p. 15
参考文献
Abe
Yakugaku Zasshi, 1955 , vol. 75, p. 159,162
Chem.Abstr., 1956 , p. 1779
Full Text Show Details
Rice; Pettit
Journal of the American Chemical Society, 1943 , vol. 76, p. 302
Full Text View citing articles Show Details
Hamor; Soine
Journal of the American Pharmaceutical Association (1912-1977), 1954 , vol. 43, p. 120,122
Full Text Show Details
Merritt; Levey; Cutter
Journal of the American Chemical Society, 1939 , vol. 61, p. 15
反应条件
chloroform
Erwaermen des Reaktionsprodukts mit Acetanhydrid und Kaliumacetat;
参考文献
Du Pont de Nemours and Co.
Patent: US2462835 , 1943 ;
反应条件
sodium hypochlorite in dichloromethane
T=-5 - 0°C; 5 h;
参考文献
Mabrour, Mahmoud; Bougrin, Khalid; Benhida, Rachid; Loupy, Andre; Soufiaoui, Mohamed
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 443 - 447