2,3,4,6-O-四苄基-D-葡萄糖合成路线 (共 97 条)
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water T=20°C; 1 h;
参考文献
Pornsuriyasak, Papapida; Demchenko, Alexei V.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6630 - 6646
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water T=20°C; 1 h;
参考文献
Pornsuriyasak, Papapida; Demchenko, Alexei V.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6630 - 6646
反应条件
N,N'-dimethyl-barbituric acid; Pd(PPh3) in tetrahydrofuran T=90°C; 24 h;
参考文献
Tsukamoto, Hirokazu; Kondo, Yoshinori
Synlett, 2003 , # 7 p. 1061 - 1063
反应条件
sulfuric acid; acetic acid in water 6 h; Reflux;
参考文献
Li, Tiehai; Guo, Lina; Zhang, Yan; Wang, Jiajia; Zhang, Zhenxing; Li, Jing; Zhang, Wenpeng; Lin, Jianping; Zhao, Wei; Wang, Peng George
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2136 - 2144
反应条件
sulfuric acid in acetic acid T=100°C; 3 h;
参考文献
Mandai, Tadakatsu; Okumoto, Hiroshi; Oshitari, Tetsuta; Nakanishi, Katsuyoshi; Mikuni, Katsuhiko; Hara, Ko-ji; Hara, Ko-zo; Iwatani, Wakao; Amano, Tetsuya; Nakamura, Kosho; Tsuchiya, Yoshinori
Heterocycles, 2001 , vol. 54, # 2 p. 561 - 566
反应条件
2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve in dichloromethane T=-78 - -60°C;
参考文献
Gildersleeve, Jeff
Journal of the American Chemical Society, 1998 , vol. 120, # 24 p. 5961 - 5969
反应条件
sulfuric acid; acetic acid Reflux;
参考文献
Fernandez-Herrera, Maria A.; Lopez-Munoz, Hugo; Hernandez-Vazquez, Jose M.V.; Lopez-Davila, Moises; Mohan, Sankar; Escobar-Sanchez, Maria L.; Sanchez-Sanchez, Luis; Pinto, B. Mario; Sandoval-Ramirez, Jesus
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 9 p. 3877 - 3886
反应条件
trifluoroacetic acid in dichloromethane T=0°C; 0.5 h;
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
trifluoroacetic acid in dichloromethane T=0°C; 4 h;
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
N-bromosuccinmide; water in acetone T=20°C; 16 h;
参考文献
Pornsuriyasak, Papapida; Demchenko, Alexei V.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6630 - 6646