甲基2-甲基-3-巯基丙酸酯合成路线 （共 8 条）
反应条件
sulfuric acid in methanol; diethyl ether
参考文献
Union Carbide Corporation
Patent: US4454134 A1, 1984 ;
反应条件
thiobenzoic S-acid; titanium tetrachloride in dichloromethane
T=-78°C; 0.333333 h;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Fujita, Tetsuhiro
Tetrahedron Letters, 1991 , vol. 32, # 46 p. 6723 - 6726
反应条件
sodium sulfide
T=0 - 5°C; 2 h;
参考文献
Vasil'eva, T. P.; Bystrova, V. M.; Kil'disheva, O. V.; Knunyats, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 6 p. 1176 - 1180
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 6 p. 1299 - 1303
反应条件
cation-exchange resin PK-216 (H type)
T=65°C; 1 h;
参考文献
Sakimae, Akihiro; Ozaki, Eiji; Toyama, Hiroko; Ohsuga, Naoto; Numazawa, Ryozo; et al.
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 5 p. 782 - 786
反应条件
piperidine; hydrogen sulfide
T=90°C;
参考文献
du Pont de Nemours and Co.
Patent: US2268185 , 1939 ;
反应条件
sodium methylate in methanol
Ambient temperature;
参考文献
Matsubara, Yoshio; Nakamura, Toshiyuki; Yoshihara, Masakuni; Maeshima, Toshihishi
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 9 p. 3389 - 3391
反应条件
thiobenzoic S-acid; n-propyl-magnesium bromide; titanium tetrachloride
1) Et2O, 0 deg C, 72 h; Yield given. Multistep reaction;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Fujita, Tetsuhiro
Tetrahedron Letters, 1991 , vol. 32, # 46 p. 6723 - 6726
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1964 , p. 600 - 605
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1964 , p. 644 - 651
