3,3'-硫代二丙酸二甲酯合成路线 （共 23 条）
反应条件
1: sodium methylate; toluene
2: aqueous sulfuric acid; acetic acid
3: diethyl ether
4: oxalic acid / Hydrieren des Reaktionsprodukts an Platin in Aethanol
View Scheme
参考文献
Onesta; Castelfranchi
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 1127,1136
反应条件
1: 13 percent / NaH, HMPA / tetrahydrofuran; paraffin / 17 h / Heating
2: 1) NaH, hexamethylphosphoramide, 2) NaI / 1) THF, mineral oil, 1 h, room temperature, 2) 4 h, reflux
3: 30 percent / n-Bu3SnH, AIBN / benzene / 1 h / Heating
View Scheme
参考文献
Dowd, Paul; Choi, Soo-Chang
Tetrahedron, 1991 , vol. 47, # 27 p. 4847 - 4860
反应条件
ammonium hydroxide in methanol
T=60°C; 4 h;
参考文献
Kumar, Anil; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 880 - 882
