双(3,4-二甲氧基苯基)甲酮合成路线 （共 39 条）
反应条件
aluminium trichloride
参考文献
Celgene Corporation
Patent: US5929117 A1, 1999 ;
反应条件
1: triethylsilane; trifluoroacetic acid / 20 °C 2: boron tribromide / dichloromethane / 4 h / 20 °C / Cooling with ice View Scheme
参考文献
Balaydin, Halis Tuerker; Durdagi, Serdar; Ekinci, Deniz; Sentuerk, Murat; Goeksu, Sueleyman; Menzek, Abdullah
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 4 p. 467 - 475
反应条件
aluminium trichloride
参考文献
Celgene Corporation
Patent: US5929117 A1, 1999 ;
反应条件
polyphosphoric acid
T=80°C; 2 h;
参考文献
Jiang, Bo; Shi, Dayong; Cui, Yongchao; Guo, Shuju
Archiv der Pharmazie, 2012 , vol. 345, # 6 p. 444 - 453
反应条件
aluminium trichloride in dichloromethane
Friedel-Crafts acylation; 2 h; Heating;
参考文献
Silvestri, Maximilian A.; Nagarajan, Muthukaman; De Clercq, Erik; Pannecouque, Christophe; Cushman, Mark
Journal of Medicinal Chemistry, 2004 , vol. 47, # 12 p. 3149 - 3162
反应条件
1: bromodifluoromethyl phenyl sulphide With AlCl3, aluminium chloride in dichloromethane
T=20°C; Friedel Crafts type alkylation; 0.25 h; Inert atmosphere;
2: 1,2-dimethoxy-benzene in dichloromethane
T=20°C; Friedel Crafts type alkylation; 16 h; Inert atmosphere;
参考文献
Kuhakarn, Chutima; Surapanich, Nakin; Kamtonwong, Siriporn; Pohmakotr, Manat; Reutrakul, Vichai
European Journal of Organic Chemistry, 2011 , # 29 p. 5911 - 5918
反应条件
acetic acid
T=30°C; 3 h;
参考文献
Jin, Yong-Sheng; Zhang, Wei; Zhang, Da-Zhi; Qiao, Li-Ming; Wu, Qiu-Ye; Chen, Hai-Sheng
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 1117 - 1119
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; copper diacetate in 1,4-dioxane
T=70°C; 2 h; Inert atmosphere;
参考文献
Kitamura, Mitsuru; Tokuda, Yu; Tashiro, Norifumi; Okauchi, Tatsuo
Australian Journal of Chemistry, 2012 , vol. 65, # 12 p. 1687 - 1690
反应条件
carbon disulfide; aluminium trichloride
参考文献
Hartwell; Kornberg
Journal of the American Chemical Society, 1945 , vol. 67, p. 1606
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Staudinger; Schlenker; Goldstein
Helvetica Chimica Acta, 1921 , vol. 4, p. 341
参考文献
Pearl
Journal of the American Chemical Society, 1954 , vol. 76, p. 3635
