2-氯-1-碘-4-硝基苯合成路线 （共 15 条）
反应条件
ueber die Diazoverbindung;
参考文献
Sato, Motohide; Kawakami, Hiroshi; Motomura, Takahisa; Aramaki, Hisateru; Matsuda, Takashi; Yamashita, Masaki; Ito, Yoshiharu; Matsuzaki, Yuji; Yamataka, Kazunobu; Ikeda, Satoru; Shinkai, Hisashi
Journal of Medicinal Chemistry, 2009 , vol. 52, # 15 p. 4869 - 4882
反应条件
tetrafluoroboric acid; hydrogen iodide in acetonitrile T=60°C; 0.5 h;
参考文献
Barbero; Degani; Diulgheroff; Dughera; Fochi
Synthesis, 2001 , # 14 p. 2180 - 2190
反应条件
1: potassium carbonate / H2O; tetrahydrofuran 2: sodium iodide; BF3*OEt2 / acetonitrile / 2 h / 40 °C View Scheme
参考文献
Saeki, Tomoyuki; Son, Eun-Cheol; Tamao, Kohei
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 9 p. 1654 - 1658
反应条件
hydrogenchloride; potassium iodide; sodium nitrite 1.) 1 h; Yield given. Multistep reaction;
参考文献
Ronaldson
Australian Journal of Chemistry, 1981 , vol. 34, # 9 p. 1935 - 1944
反应条件
KIO3; sulfuric acid; iodine
参考文献
Arotsky,J. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1973 , p. 595 - 599
反应条件
1: alcohol; ammonia 2: ueber die Diazoverbindung View Scheme
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1913 , vol. <5> 22 I, p. 823
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1914 , vol. <5> 23 I, p. 283 Anm.
参考文献
Wallagh; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 1071,1073
参考文献
Bloom, Jonathan D.; DiGrandi, Martin J.; Dushin, Russell G.; Curran, Kevin J.; Ross, Adma A.; Norton, Emily B.; Terefenko, Eugene; Jones, Thomas R.; Feld, Boris; Lang, Stanley A.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 17 p. 2929 - 2932
反应条件
1: 210 - 215 °C 2: SnCl2, aq. HCl 3: (i) NaNO2, aq. HCl, (ii) CuCl View Scheme
参考文献
Pan; Fletcher
Journal of medicinal chemistry, 1965 , vol. 8, # 4 p. 491 - 497
参考文献
Pan; Fletcher
Journal of medicinal chemistry, 1965 , vol. 8, # 4 p. 491 - 497
