N-苄氧羰基-L-谷氨酸酐合成路线 （共 62 条）
反应条件
1: chloroform / anfangs unter Kuehlung 2: chloroform; PCl5 / -5 °C / Behandeln des Reaktionsprodukts mit aether. NH3 3: aq.-ethanolic NaOH View Scheme
参考文献
Melville
Biochemical Journal, 1935 , vol. 29, p. 179,182
反应条件
benzyl alcohol T=100°C;
参考文献
Bergmann; Zervas; Salzmann
Chemische Berichte, 1933 , vol. 66, p. 1288,1290
参考文献
Weygand,F.; Hunger,K.
Chemische Berichte, 1962 , vol. 95, p. 7 - 16
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Losse,G. et al.
Chemische Berichte, 1963 , vol. 96, p. 204 - 212
反应条件
1: dicyclohexylamine (DCHA) / tetrahydrofuran / 0 °C 2: 70percent perchloric acid / Ambient temperature 3: 100 percent / 1 M KOH / methanol View Scheme
参考文献
Dolence, E. Kurt; Lin, Chia-En; Miller, Marvin J.; Payne, Shelley M.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 3 p. 956 - 968
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without DMAP; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
diethyl ether; N,N-dicyclohexylamine
参考文献
Napolitano, Roberta; Pariani, Giorgio; Fedeli, Franco; Baranyai, Zsolt; Aswendt, Markus; Aime, Silvio; Gianolio, Eliana
Journal of Medicinal Chemistry, 2013 , vol. 56, # 6 p. 2466 - 2477
参考文献
Harington; Mead
Biochemical Journal, 1935 , vol. 29, p. 1602,1605
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du Vigneaud; Miller
Biochemical Preparations, 1952 , vol. 2, p. 74,75
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Sorm; Rudinger
Collection of Czechoslovak Chemical Communications, 1950 , vol. 15, p. 491,493
参考文献
Klieger,E.; Gibian,H.
Justus Liebigs Annalen der Chemie, 1962 , vol. 655, p. 195 - 210
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Le Quesne; Young
Journal of the Chemical Society, 1950 , p. 1954,1958
反应条件
1: dicyclohexylamine; diethyl ether 2: H2 / Pd View Scheme
参考文献
Klieger,E.; Gibian,H.
Justus Liebigs Annalen der Chemie, 1962 , vol. 655, p. 195 - 210
反应条件
anschliessendes Hydrieren;
参考文献
Matsukawa; Masuda
Yakugaku Zasshi, 1953 , vol. 73, p. 397
Chem.Abstr., 1954 , p. 2597
