N1,N1-二(4-氨基苯基)苯-1,4-二胺合成路线 （共 7 条）
反应条件
palladium 10 on activated carbon; hydrazine hydrate in ethanol
T=120°C; 8 h;
参考文献
Bae, Jun; Chae, Boknam; Seo, Hyemi; Jung, Young Mee; Lee, Seung Woo
Journal of Molecular Structure, 2014 , vol. 1069, # 1 p. 200 - 204
反应条件
1: 41 percent / potassium carbonate / dimethylsulfoxide / 48 h / Heating
2: 51 percent / hydrazine monohydrate / Pd/C / ethanol / 24 h / Heating
View Scheme
参考文献
Ling, Qi-Dan; Chang, Feng-Chyuan; Song, Yan; Zhu, Chun-Xiang; Liaw, Der-Jang; Chan, Daniel Siu-Hhung; Kang, En-Tang; Neoh, Koon-Gee
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8732 - 8733
反应条件
1: CsF
2: hydrazine / Pd/C
View Scheme
参考文献
Cheng, Shu-Hua; Hsiao, Sheng-Huei; Su, Tzy-Hsiang; Liou, Guey-Sheng
Macromolecules, 2005 , vol. 38, # 2 p. 307 - 316
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Chang, Cha-Wen; Liou, Guey-Sheng; Hsiao, Sheng-Huei
Journal of Materials Chemistry, 2007 , vol. 17, # 10 p. 1007 - 1015
反应条件
1: 41 percent / potassium carbonate / dimethylsulfoxide / 48 h / Heating
2: 51 percent / hydrazine monohydrate / Pd/C / ethanol / 24 h / Heating
View Scheme
参考文献
Ling, Qi-Dan; Chang, Feng-Chyuan; Song, Yan; Zhu, Chun-Xiang; Liaw, Der-Jang; Chan, Daniel Siu-Hhung; Kang, En-Tang; Neoh, Koon-Gee
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8732 - 8733
反应条件
potassium carbonate; aniline in water; N,N-dimethyl-formamide
参考文献
Idemitsu Kosan Co., Ltd.
Patent: US6074734 A1, 2000 ;
反应条件
1.1: sodium hydride / N,N-dimethyl acetamide / 0.5 h / 20 °C
1.2: 1 h / 100 °C
2.1: 10 palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
View Scheme
参考文献
Lee, Wen-Ya; Kurosawa, Tadanori; Lin, Shiang-Tai; Higashihara, Tomoya; Ueda, Mitsuru; Chen, Wen-Chang
Chemistry of Materials, 2011 , vol. 23, # 20 p. 4487 - 4497
反应条件
1: glacial acetic acid; nitric acid / 55 - 60 °C / man laesst 2 Stdn. bei 27-28grad stehen
2: tin; hydrochloric acid
View Scheme
参考文献
Herz
Chemische Berichte, 1890 , vol. 23, p. 2537
