反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 1.5 h / -5 °C
1.2: 90 percent / hexamethylphosphoric acid triamide; tetrahydrofuran; hexane / 10 h / 20 °C
2.1: HF / acetonitrile / 0.5 h / 20 °C
3.1: 76 percent / 2,2,6,6-tetramethylpiperidine 1-oxyl; NaClO; NaClO2 / acetonitrile; H2O / 5 h / 37 °C / pH 6.86
View Scheme
参考文献
Koseki, Yuji; Kusano, Shuichi; Ichi, Daisuke; Yoshida, Keiji; Nagasaka, Tatsuo
Tetrahedron, 2000 , vol. 56, # 45 p. 8855 - 8865
