1-苯基-1,3,4,5-四氢苯并[cd]吲唑合成路线 （共 3 条）
反应条件
1: 34 percent / n-BuLi; TMEDA / pentane; hexane / -78 - 20 °C
2: 41 percent / CrO3; AcOH / H2O / 12 h / 20 °C
3: 62 percent / diethyl ether / 140 h / 40 °C
4: 40 percent / K3PO4; Pd(dba)2; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 110 °C
View Scheme
参考文献
Lebedev, Artyom Y.; Khartulyari, Anton S.; Voskoboynikov, Alexander Z.
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 596 - 602
反应条件
1: 62 percent / diethyl ether / 140 h / 40 °C
2: 40 percent / K3PO4; Pd(dba)2; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 110 °C
View Scheme
参考文献
Lebedev, Artyom Y.; Khartulyari, Anton S.; Voskoboynikov, Alexander Z.
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 596 - 602
反应条件
1: 41 percent / CrO3; AcOH / H2O / 12 h / 20 °C
2: 62 percent / diethyl ether / 140 h / 40 °C
3: 40 percent / K3PO4; Pd(dba)2; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 110 °C
View Scheme
参考文献
Lebedev, Artyom Y.; Khartulyari, Anton S.; Voskoboynikov, Alexander Z.
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 596 - 602
