1,2-o-异亚丙基-3-苯甲酰基氧基-5,6-二脱氧-呋喃葡萄糖合成路线 （共 5 条）
反应条件
1H-imidazole; iodine; triphenylphosphine in toluene
5 h; Heating;
参考文献
Biswas, Goutam; Sengupta, Jhimli; Nath, Madhumita; Bhattacharjya, Anup
Carbohydrate Research, 2005 , vol. 340, # 4 p. 567 - 578
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene
T=10 - 15°C; 4 h; Irradiation; Further byproducts given;
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
反应条件
1: 89 percent / pyridine
2: 6.1 percent / (Bu3Sn)2 / benzene / 4 h / 10 - 15 °C / Irradiation
View Scheme
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
反应条件
1: 1.) Bu2SnO / 1.) MeOH, reflux, 3 h, 2.) dioxane, from 5 deg C to 10 deg C, 1 h
2: 89 percent / pyridine
3: 6.1 percent / (Bu3Sn)2 / benzene / 4 h / 10 - 15 °C / Irradiation
View Scheme
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
反应条件
lithium hydroxide in methanol; water
T=25°C; 12 h;
参考文献
Biswas, Goutam; Sengupta, Jhimli; Nath, Madhumita; Bhattacharjya, Anup
Carbohydrate Research, 2005 , vol. 340, # 4 p. 567 - 578
