甲基-2,3-O-异亚丙基-beta-D-呋喃核糖苷合成路线 （共 77 条）
反应条件
1: With aluminium trifluoromethanesulphonate in methanol T=20 - 25°C; 2 h; Inert atmosphere; 2: With water; sodium hydrogencarbonate in methanol; dichloromethane T=20 - 25°C; Inert atmosphere;
参考文献
Williams, D. Bradley G.; Simelane, Sandile B.; Lawton, Michelle; Kinfe, Henok H.
Tetrahedron, 2010 , vol. 66, # 25 p. 4573 - 4576
反应条件
1: With aluminium trifluoromethanesulphonate in methanol T=20 - 25°C; 2 h; Inert atmosphere; 2: With water; sodium hydrogencarbonate in methanol; dichloromethane T=20 - 25°C; Inert atmosphere;
参考文献
Williams, D. Bradley G.; Simelane, Sandile B.; Lawton, Michelle; Kinfe, Henok H.
Tetrahedron, 2010 , vol. 66, # 25 p. 4573 - 4576
反应条件
hydrogenchloride in acetone
参考文献
Abdel-Rahman, Adel A.-H.; Abdel-Megied, Ahmed E.-S.; Goda, Adel E.-S.; Zeid, Ibrahim F.; El Ashry, El Sayed H.
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 11 p. 2027 - 2038
反应条件
1: With hydrogenchloride in methanol; acetone T=20°C; 21 h; 2: With pyridine in acetone Further stages.;
参考文献
Palmer, Andreas M.; Jaeger, Volker
European Journal of Organic Chemistry, 2001 , # 7 p. 1293 - 1308
反应条件
sulfuric acid T=20°C; Inert atmosphere;
参考文献
Ferreira, Sabrinab; Sodero, Ana C. R.; Cardoso, Mariana F. C.; Lima, Emerson S.; Kaiser, Carlos R.; Silva Jr., Floriano P.; Ferreira, Vitor F.
Journal of Medicinal Chemistry, 2010 , vol. 53, # 6 p. 2364 - 2375
反应条件
1: With ozone in methanol T=-78°C; 0.5 h; 2: With sodium tetrahydroborate in methanol T=0 - 20°C;
参考文献
Awasaguchi, Ken-Ichiro; Miyazawa, Masahiro; Uoya, Ikuyo; Inoue, Koichi; Nakamura, Koji; Yokoyama, Hajime; Hirai, Yoshiro
Heterocycles, 2010 , vol. 81, # 9 p. 2105 - 2121
反应条件
lithium aluminium tetrahydride in diethyl ether 0.416667 h; Heating; Yield given;
参考文献
Ito, Yukishige; Shibata, Tomoyuki; Arita, Masafumi; Sawai, Hiroaki; Ohno, Masaji
Journal of the American Chemical Society, 1981 , vol. 103, # 22 p. 6739 - 6741
反应条件
1: HCl / Ambient temperature 2: LiAlH4 / diethyl ether View Scheme
参考文献
Ohno, Masaji; Ito, Yukishige; Arita, Masafumi; Shibata, Tomoyuki; Adachi, Kunitomo; Sawai, Hiroaki
Tetrahedron, 1984 , vol. 40, # 1 p. 145 - 152
反应条件
camphor-10-sulfonic acid in acetone 22 h; Ambient temperature;
参考文献
Francesconi, Kevin A.; Edmonds, John S.; Stick, Robert V.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 11 p. 2707 - 2716
反应条件
anhydrous cadmium carbonate; mercury dichloride in methanol 19 h; Heating;
参考文献
Yamamoto, Hiroshi; Nakamura, Yuhji; Kawamoto, Heizan; Inokawa, Saburo; Yamashita, Mitsuji; et al.
Carbohydrate Research, 1982 , vol. 102, p. 185 - 196
