甲基-2,3-O-异亚丙基-beta-D-呋喃核糖苷合成路线 （共 77 条）
反应条件
hydrogenchloride in methanol T=20°C;
参考文献
Gosselin, Gilles; Imbach, Jean-Louis; Sommadossi, Jean-Pierre
Patent: US2004/6007 A1, 2004 ;
Location in patent: Page/Page column 18; sheet 2 ;
反应条件
in acetone T=20°C; 16 h;
参考文献
Coll Farma S.L.
Patent: EP2241556 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogenchloride in methanol; dichloromethane; water; acetone
参考文献
Sommadossi, Jean-Pierre; Gosselin, Gilles; Imbach, Jean-Louis
Patent: US2004/6002 A1, 2004 ;
反应条件
acetyl chloride in methanol 12 h; Inert atmosphereReflux;
参考文献
Ting, Samuel Z.Y.; Baird, Lynton J.; Dunn, Elyse; Hanna, Reem; Leahy, Dora; Chan, Ariane; Miller, John H.; Teesdale-Spittle, Paul H.; Harvey, Joanne E.
Tetrahedron, 2013 , vol. 69, # 49 p. 10581 - 10592
反应条件
hydrogenchloride in acetone T=20°C;
参考文献
van Tilburg; van der Klein; von Frijtag Drabbe Kuenzel; de Groote; Stannek; Lorenzen; IJzerman
Journal of medicinal chemistry, 2001 , vol. 44, # 18 p. 2966 - 2975
反应条件
hydrogenchloride in water 1 h; Reflux;
参考文献
Davies, Stephen G.; Durbin, Matthew J.; Goddard, Euan C.; Kelly, Peter M.; Kurosawa, Wataru; Lee, James A.; Nicholson, Rebecca L.; Price, Paul D.; Roberts, Paul M.; Russell, Angela J.; Scott, Philip M.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 4 p. 761 - 776
反应条件
sulfuric acid; tin(ll) chloride T=40 - 45°C; 20 h;
参考文献
Sairam, Pothukuchi; Puranik, Ramachandra; Sreenivasa Rao, Bhatraju; Veerabhadra Swamy, Ponnapalli; Chandra, Sharad
Carbohydrate Research, 2003 , vol. 338, # 4 p. 303 - 306
反应条件
silver hexafluoroantimonate; phloroglucinol trimethyl ether in dichloromethane T=40°C; 2 h;
参考文献
Kern, Nicolas; Dombray, Thomas; Blanc, Aurelien; Weibel, Jean-Marc; Pale, Patrick
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9227 - 9235,9
反应条件
cyclohexene; palladium dihydroxide in ethanol 2 h; Heating;
参考文献
Hanessian, Stephen; Liak, Teng Jiam; Vanasse, Benoit
Synthesis, 1981 , # 5 p. 396 - 397
反应条件
lithium aluminium tetrahydride; lithium diisopropyl amide in tetrahydrofuran T=-30°C; Reduction;
参考文献
Stepowska, Halszka; Zamojski, Aleksander
Carbohydrate Research, 1999 , vol. 321, # 1-2 p. 105 - 109
