1-(噻唑-2-基)乙醇合成路线 (共 10 条)
反应条件
1: acetic acid; aqueous Na2Cr2O7 2: CCl4; bromine View Scheme
参考文献
Erlenmeyer et al.
Helvetica Chimica Acta, 1948 , vol. 31, p. 1142,1156
反应条件
sodium dichromate in water; acetic acid 1 h; Heating;
参考文献
Jones, Gurnos; Ollivierre, Hermione; Fuller, L. S.; Young, J. H.
Tetrahedron, 1991 , vol. 47, # 16 p. 2851 - 2860
反应条件
Sphingomonas paucimobilis NCIMB 8195 in water; N,N-dimethyl-formamide 120 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 19 p. 6495 - 6497
反应条件
zirconium(IV) hydrous oxide hydroxide; isopropyl alcohol
T=130°C; Meerwein-Ponndorf-Verley Reduction; 0.583333 h;
参考文献
Battilocchio, Claudio; Hawkins, Joel M.; Ley, Steven V.
Organic Letters, 2013 , vol. 15, # 9 p. 2278 - 2281
反应条件
(i) nBuLi, (ii) /BRN= 505984/; Multistep reaction;
参考文献
Noyce,D.S.; Fike,S.A.
Journal of Organic Chemistry, 1973 , vol. 38, p. 3316 - 3318
反应条件
sulfuric acid
2.5 h; Heating;
参考文献
Jones, Gurnos; Ollivierre, Hermione; Fuller, L. S.; Young, J. H.
Tetrahedron, 1991 , vol. 47, # 16 p. 2851 - 2860
参考文献
Allevi, Pietro; Ciuffreda, Pierangela; Tarocco, Giorgio; Anastasia, Mario
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 4144 - 4147
反应条件
sulfuric acid
Heating;
参考文献
Jones, Gurnos; Ollivierre, Hermione; Fuller; Young
Tetrahedron, 1991 , vol. 47, # 16-17 p. 2861 - 2870
反应条件
1: 75 percent / nickel peroxide / CH2Cl2
2: 80 percent / 2M H2SO4 / 2.5 h / Heating
View Scheme
参考文献
Jones, Gurnos; Ollivierre, Hermione; Fuller, L. S.; Young, J. H.
Tetrahedron, 1991 , vol. 47, # 16 p. 2851 - 2860
参考文献
NEUROCRINE BIOSCIENCES, INC.
Patent: WO2005/97093 A1, 2005 ;
Location in patent: Page/Page column 65 ;