4-叔丁基-2,6-二硝基苯酚合成路线 (共 9 条)
反应条件
nitric acid in acetic acid from -15 deg C to RT over 30 min;
参考文献
Rojo, Javier; Lehn, Jean-Marie; Baum, Gerhard; Fenske, Dieter; Waldmann, Oliver; Mueller, Paul
European Journal of Inorganic Chemistry, 1999 , # 3 p. 517 - 522
反应条件
Montmorillonite KSF; nitric acid; hafnium oxychloride in tetrahydrofuran T=20°C; 16 h;
参考文献
Shi, Min; Cui, Shi-Cong; Yin, Wan-Po
European Journal of Organic Chemistry, 2005 , # 11 p. 2379 - 2384
反应条件
sulfuric acid T=60 - 70°C; Eintragen des Reaktionsgemisches in Wasser und anschliessendes Erwaermen mit Salpetersaeure auf 70-80grad;
参考文献
Hart
Journal of the American Chemical Society, 1949 , vol. 71, p. 1966
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Dow Chem. Co.
Patent: US2192197 , 1936 ;
反应条件
T=60 - 70°C; Eintragen des Reaktionsgemisches in Wasser und anschliessendes Erwaermen mit wss. HNO3 auf 70-80grad;
参考文献
Hart
Journal of the American Chemical Society, 1949 , vol. 71, p. 1966
Full Text View citing articles Show Details
Dow. Chem. Co.
Patent: US2192197 , 1936 ;
参考文献
Tierie
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 126
Full Text Show Details
Schaaf
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2> 133, p. 173
反应条件
1-methyl-1H-imidazole in toluene
参考文献
Union Carbide Corporation
Patent: US4395572 A1, 1983 ;
反应条件
sodium hydroxide in methanol; water
参考文献
Amchem Products, Inc.
Patent: US3991116 A1, 1976 ;
参考文献
Jedlicka
Journal fuer Praktische Chemie (Leipzig), 1893 , vol. <2>48, p. 103
反应条件
thionyl chloride; N,N-dimethyl-formamide in toluene 8 h; Heating / reflux;
参考文献
KEMIA, INC.
Patent: WO2008/89034 A2, 2008 ;
Location in patent: Page/Page column 123 ;