5-甲氧基-3H-苯并恶唑-2-酮合成路线 （共 14 条）
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 1.16667 h; Inert atmosphere;
参考文献
YALE UNIVERSITY; JORGENSEN, William; BUCALA, Richard, J.
Patent: WO2010/21693 A2, 2010 ;
Location in patent: Page/Page column 34 ;
反应条件
selenium; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine in toluene
T=150°C; P=22800 Torr; 7 h;
参考文献
Wang, Xiaofang; Ling, Gang; Xue, Yan; Lu, Shiwei
European Journal of Organic Chemistry, 2005 , # 8 p. 1675 - 1679
反应条件
in tetrahydrofuran
T=20°C; 1 h;
参考文献
MERCK PATENT GESELLSCHAFT MIT BESCHRANKTER HAFTUNG
Patent: US2010/280030 A1, 2010 ;
Location in patent: Page/Page column 19 ;
参考文献
Nikam, Sham Shridhar; Scott, Ian Leslie; Sherer, Brian Alan; Wise, Lawrence David
Patent: US2003/236252 A1, 2003 ;
Location in patent: Page 50 ;
反应条件
sodium azide; iodine; sodium hydrogencarbonate in N,N-dimethyl-formamide
T=100°C; 2 h;
参考文献
Rajendar; Kant, Ruchir; Narender
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3591 - 3596
反应条件
polymer-supported diphenylphosphoryl azide; triethylamine in benzene
24 h; Heating;
参考文献
Lu, Yuhua; Taylor, Richard T.
Heterocycles, 2004 , vol. 62, p. 869 - 876
反应条件
2: aqueous NaOH-solution; sodium dithionite
View Scheme
参考文献
Close; Tiffany; Spielman
Journal of the American Chemical Society, 1949 , vol. 71, p. 1265,1266
反应条件
1: aqueous NaOH-solution; sodium dithionite
View Scheme
参考文献
Close; Tiffany; Spielman
Journal of the American Chemical Society, 1949 , vol. 71, p. 1265,1266
反应条件
1: (i) MeOH, (ii) H2O
2: aq. HCl / Heating
View Scheme
参考文献
Sam,J.; Plampin,J.N.
Journal of Pharmaceutical Sciences, 1964 , vol. 53, p. 538 - 544
反应条件
1: PbO / methanol / Heating
2: aq. HCl / Heating
View Scheme
参考文献
Sam,J.; Plampin,J.N.
Journal of Pharmaceutical Sciences, 1964 , vol. 53, p. 538 - 544
