N-甲基-4-甲氧基-beta-苯乙胺合成路线 (共 17 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Heating;
参考文献
Xu, Wei; Zhang, Xiao-Ming; Mariano, Patrick S.
Journal of the American Chemical Society, 1991 , vol. 113, # 23 p. 8863 - 8878
反应条件
1: With Ind2TiMe2 in toluene T=80°C; P=760 Torr; 7 h; 2: With sodium cyanoborohydride; zinc(II) chloride in methanol; toluene T=25°C; 16 h;
参考文献
Marcsekova, Klaudia; Wegener, Bernd; Doye, Sven
European Journal of Organic Chemistry, 2005 , # 22 p. 4843 - 4851
反应条件
1: 99 percent / K2CO3 / tetrahydrofuran / 25 °C 2: 99 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme
参考文献
Lagarias; Houghten; Rapoport
Journal of the American Chemical Society, 1978 , vol. 100, # 26 p. 8202 - 8209
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Lagarias; Houghten; Rapoport
Journal of the American Chemical Society, 1978 , vol. 100, # 26 p. 8202 - 8209
反应条件
1: (catalytic hydrogenation) 2: Et3N / CHCl3 3: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Lagarias; Houghten; Rapoport
Journal of the American Chemical Society, 1978 , vol. 100, # 26 p. 8202 - 8209
反应条件
in methanol 168 h; Ambient temperature;
参考文献
Katsu; Ono; Tasaka; Fujita
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 4185 - 4188
参考文献
La Forge; Barthel
Journal of Organic Chemistry, 1941 , vol. 9, p. 250,252
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Nani, Roger R.; Reisman, Sarah E.
Journal of the American Chemical Society, 2013 , vol. 135, # 19 p. 7304 - 7311
反应条件
1: SOCl2 / 0.5 h / Heating 2: 73 percent / methanol / 168 h / Ambient temperature View Scheme
参考文献
Katsu; Ono; Tasaka; Fujita
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 4185 - 4188
反应条件
1: toluene; water / 0.5 h / 0 - 22 °C / |Inert atmosphere 2: borane-THF / tetrahydrofuran / 4 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Nani, Roger R.; Reisman, Sarah E.
Journal of the American Chemical Society, 2013 , vol. 135, # 19 p. 7304 - 7311