2,2'-氧基二[5,5-二甲基-1,3,2-二氧杂磷杂环己烷] 2,2'-二氧化物合成路线 （共 10 条）
反应条件
trichlorophosphate in toluene
T=50 - 75°C; 2 h;
参考文献
DAIHACHI CHEMICAL INDUSTRY CO., LTD.
Patent: EP1808437 A1, 2007 ;
Location in patent: Page/Page column 13-14; 17 ;
反应条件
N,N,N',N,-tetramethylethylenediamine; copper(ll) bromide in tetrahydrofuran
T=25°C; 24 h;
参考文献
Zhou, Yongbo; Yin, Shuangfeng; Gao, Yuxing; Zhao, Yufen; Goto, Midori; Han, Li-Biao
Angewandte Chemie - International Edition, 2010 , vol. 49, # 38 p. 6852 - 6855
反应条件
benzenephosphonous acid; sodium hydride in tetrahydrofuran
T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Nycz
Polish Journal of Chemistry, 2009 , vol. 83, # 4 p. 589 - 594
反应条件
in toluene
T=25°C; Yields of byproduct given;
参考文献
Vijjulatha; Praveen Kumar; Kumara Swamy; Vittal
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1819 - 1822
反应条件
iodosylbenzene in tetrahydrofuran
12 h; Heating;
参考文献
Makowiec, Slawomir; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 4 p. 941 - 955
反应条件
benzenephosphonous acid; sodium hydride in tetrahydrofuran
T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Nycz
Polish Journal of Chemistry, 2009 , vol. 83, # 4 p. 589 - 594
反应条件
1: 63 percent
2: 52 percent / benzene
3: pyridine
View Scheme
参考文献
Baraniak; Stec
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 137 - 140
反应条件
1: 52 percent / benzene
2: pyridine
View Scheme
参考文献
Baraniak; Stec
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 137 - 140
参考文献
Baraniak; Stec
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 137 - 140
反应条件
in xylene
T=120°C; 24 h; other temperature; Product distributionMechanism;
参考文献
Cullis, Paul M.; Kay, Paul B.; Trippett, Stuart
Journal of the Chemical Society, Chemical Communications, 1985 , # 19 p. 1329 - 1331
