1-(2-硝基苯基)-吡咯烷合成路线 (共 8 条)
反应条件
hydrogen; palladium 10 on activated carbon in ethanol T=20°C; 20 h;
参考文献
DEVELOGEN AKTIENGESELLSCHAFT
Patent: WO2006/136402 A1, 2006 ;
Location in patent: Page/Page column 89-90 ;
WO 2006/136402 A1
反应条件
in tetrahydrofuran
T=50°C; P=6375510 Torr; 20 h;
参考文献
Ibata, Toshikazu; Isogami, Yasushi; Toyoda, Jiro
Chemistry Letters, 1987 , p. 1187 - 1190
反应条件
in tetrahydrofuran
T=50°C; P=5400430 Torr; 20 h;
参考文献
DEVELOGEN AKTIENGESELLSCHAFT
Patent: WO2006/136402 A1, 2006 ;
Location in patent: Page/Page column 89 ;
WO 2006/136402 A1
反应条件
solid-supported nano and microparticles of Pd(0) in N,N-dimethyl-formamide
T=80°C; 4 h;
参考文献
Bandna; Guha, Nitul Ranjan; Shil, Arun K.; Sharma, Dharminder; Das, Pralay
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5318 - 5322
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yields of byproduct given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
in tetrahydrofuran
T=80°C; P=5625450 Torr; 20 h;
参考文献
Ibata, Toshikazu; Shang, Muhong; Demura, Tetsuo
Chemistry Letters, 1994 , # 2 p. 359 - 362
Title/Abstract Full Text Show Details
Ibata, Toshikazu; Shang, Muhong; Demura, Tetsuo
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 9 p. 2717 - 2726
参考文献
Liu, Wei; Ma, Yuan; Yin, Yingwu; Zhao, Yufen
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 4 p. 577 - 579
反应条件
hexamethyl-silane; tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad
Tetrahedron Letters, 1984 , vol. 25, # 12 p. 1259 - 1262