4'-正戊基-4-氰基联苯合成路线 （共 23 条）
反应条件
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature 2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h 3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h 4: 73 percent / acetic anhydride / 2 h / Heating View Scheme
参考文献
Dabrowski; Witkiewicz; Kenig
Molecular crystals and liquid crystals, 1980 , vol. 58, # 3-4 p. 251 - 259
反应条件
sulfuric acid in acetic acid T=120°C;
参考文献
Kelly, Stephen M.; Huynh-Ba, Tuong
Helvetica Chimica Acta, 1983 , vol. 66, # 6 p. 1850 - 1859
反应条件
sulfuric acid; diisobutylaluminium hydride in water; ethyl acetate; toluene
参考文献
Hoffmann-La Roche Inc.
Patent: US4528114 A1, 1985 ;
反应条件
1: NaOH / ethane-1,2-diol
2: aq. H2SO4, aq. H3BO3
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: aq. H2SO4, aq. H3BO3
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: aq. H2SO4, aq. H3BO3
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: aq. H2SO4, aq. H3BO3
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: (i) SOCl2, (ii) /BRN= 507924/, Py
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: (i) SOCl2, (ii) /BRN= 1907114/, Py
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
反应条件
1: NaOH / ethane-1,2-diol
2: (i) SOCl2, (ii) /BRN= 386979/, Py
View Scheme
参考文献
Merck
Patent: FR2288732DE2450088 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 46219
