1-辛基吡咯-2,5-二酮合成路线 (共 3 条)
反应条件
1: in benzene T=30°C; 1 h; 2: With 1,1,1,3,3,3-hexamethyl-disilazane; zinc dibromide in benzene 2 h; Heating; Further stages.;
参考文献
Facchetti, Antonio; Marks, Tobin J.; Wang, Zhiming M.
Patent: US2008/185555 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
sodium acetate; acetic anhydride T=90°C; 2 h;
参考文献
Kalgutkar, Amit S.; Crews, Brenda C.; Marnett, Lawrence J.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 8 p. 1692 - 1703
反应条件
1: diethyl ether / 3 h 2: 151 mg / acetic anhydride; triethylamine / butan-2-one / 72 h / Heating View Scheme
参考文献
Uchoa, Adjaci F.; De Oliveira, Kleber T.; Baptista, Mauricio S.; Bortoluzzi, Adailton J.; Iamamoto, Yassuko; Serra, Osvaldo A.
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8824 - 8832