N,N-二甲基-2-苯并噻唑胺合成路线 （共 32 条）
反应条件
in benzene 24 h; Heating; Yield given;
参考文献
Benassi, Rois; Grandi, Romano; Pagnoni, Ugo M.; Taddei, Ferdinando; Bocelli, Gabriele; Sgarabotto, Paolo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1513 - 1522
反应条件
4-methyl-benzoic acid; silver carbonate
T=130°C; 12 h; regioselective reaction;
参考文献
Cho, Seung Hwan; Kim, Ji Young; Lee, S. Yunmi; Chang, Sukbok
Angewandte Chemie - International Edition, 2009 , vol. 48, # 48 p. 9127 - 9130
反应条件
t-BuXPhos Pd(II) phenethylamine chloride; lithium hexamethyldisilazane in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Lee, Brian K.; Biscoe, Mark R.; Buchwald, Stephen L.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3672 - 3674
反应条件
ammonia in water
T=240°C; 0.5 h;
参考文献
Petersen, Trine P.; Larsen, Anders Foller; Ritzen, Andreas; Ulven, Trond
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4190 - 4195
反应条件
in tetrahydrofuran
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in toluene
T=110°C; 0.233333 h; Inert atmosphere; Time;
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
in tetrahydrofuran
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
Ni(PEt3)2Cl2; sodium cyanoborohydride in N,N-dimethyl-formamide
T=100°C; 20 h;
参考文献
Takagi, Kentaro
Chemistry Letters, 1986 , p. 265 - 266
反应条件
1: With triethylamine in chloroform
T=-30 - -20°C;
2: With silica gel in chloroform
T=20°C; 4.5 h;
参考文献
Ohno, Kosei; Ishida, Wakako; Kamata, Kazuyuki; Oda, Kazuaki; Machida, Minoru
Heterocycles, 2003 , vol. 59, # 1 p. 317 - 322
反应条件
caesium carbonate; copper(I) bromide in dimethyl sulfoxide
T=120°C; 24 h;
参考文献
Pi, Sha-Sha; Zhang, Xing-Guo; Tang, Ri-Yuan; Li, Jin-Heng
Synlett, 2009 , # 18 p. 3032 - 3036
