4-正十二烷氧基苯甲酸甲酯合成路线 （共 14 条）
反应条件
sulfuric acid
Heating;
参考文献
Cohen, Yael; Bodner, Efrat; Richman, Michal; Afri, Michal; Frimer, Aryeh A.
Chemistry and Physics of Lipids, 2008 , vol. 155, # 2 p. 98 - 113
反应条件
1: potassium hydroxide / ethanol; water / 2 h / |Reflux
2: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
3: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
4: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: KOH / ethanol / Heating
2: DCC; DMAP / CH2Cl2
View Scheme
参考文献
Kalaivani; Narasimhaswamy; Das, Bibhuti B.; Lobo, Nitin P.; Ramanathan
Journal of Physical Chemistry B, 2011 , vol. 115, # 40 p. 11554 - 11565
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 1 h;
参考文献
Ahmed, Saleh A.; Tanaka, Mutsuo
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9884 - 9886
