1,2-双(叔丁基氨基)乙烷合成路线 （共 14 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol 3 h;
参考文献
Dieck, Heindirk tom; Verfuerth, Uwe; Diblitz, Klaus; Ehlers, Jens; Fendesak, Gert
Chemische Berichte, 1989 , vol. 122, p. 129 - 132
反应条件
in hexane; water 72 h; Heating;
参考文献
Haaf; Schmedake; Paradise; West
Canadian Journal of Chemistry, 2000 , vol. 78, # 11 p. 1526 - 1533
反应条件
lithium aluminium tetrahydride T=0 - 20°C;
参考文献
Ledoux, Nele; Allaert, Bart; Pattyn, Siegfried; Mierde, Hans Vander; Vercaemst, Carl; Verpoort, Francis
Chemistry - A European Journal, 2006 , vol. 12, # 17 p. 4654 - 4661
反应条件
hydrogen; palladium on activated charcoal in ethanol 1.5 h;
参考文献
Dieck, Heindirk tom; Verfuerth, Uwe; Diblitz, Klaus; Ehlers, Jens; Fendesak, Gert
Chemische Berichte, 1989 , vol. 122, p. 129 - 132
反应条件
in water T=20°C; 72 h;
参考文献
Denk, Michael K.; Krause, Mike J.; Niyogi, Debyani F.; Gill, Nachhattarpal K.
Tetrahedron, 2003 , vol. 59, # 38 p. 7565 - 7570
参考文献
Tilley,J.N.; Sayigh,A.A.R.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2076 - 2079
反应条件
Et3N byproducts: Et3NHCl; elem. anal.;
参考文献
Herrmann, Wolfgang A.; Denk, Michael; Behm, Joachim; Scherer, Wolfgang; Klingan, Franz-Robert; et al.
Angewandte Chemie, 1992 , vol. 104, # 11 p. 1489 - 1492
反应条件
1: SO2Cl2 / CHCl3
2: CF3CO2H / Ambient temperature
View Scheme
参考文献
Preiss,M.
Chemische Berichte, 1978 , vol. 111, p. 1915 - 1921
反应条件
1: SO2Cl2 / CHCl3
2: CF3CO2H / Ambient temperature
3: NaOH / ethanol
View Scheme
参考文献
Preiss,M.
Chemische Berichte, 1978 , vol. 111, p. 1915 - 1921
反应条件
triethylamine; phosphorus trichoride in toluene
T=20°C; 2 h;
参考文献
Krysiak, Jerzy; Lyon, Celine; Baceiredo, Antoine; Gornitzka, Heinz; Mikolajczyk, Marian; Bertrand, Guy
Chemistry - A European Journal, 2004 , vol. 10, # 8 p. 1982 - 1986
